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学科主题: 药学
题名:
Structure elucidation of a novel group of dithiocarbamate derivatives using 1D and 2D NMR spectroscopy
作者: Li, Q1; Yang, CH1; Ge, ZM1; Li, RT1; Cui, YX1
关键词: NMR ; H-1 NMR ; C-13 NMR ; 2D NMR ; structural elucidation ; dithiocarbamates
刊名: MAGNETIC RESONANCE IN CHEMISTRY
发表日期: 2006-07-01
DOI: 10.1002/mrc.1808
卷: 44, 期:7, 页:720-723
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology
类目[WOS]: Chemistry, Multidisciplinary ; Chemistry, Physical ; Spectroscopy
研究领域[WOS]: Chemistry ; Spectroscopy
关键词[WOS]: CANCER
英文摘要:

Compounds 1-7 form a novel group of dithiocarbamates, first synthesized from the reaction of a series of primary amines with carbon disulfide and 3-bromo ethyl pyruvate in the presence of anhydrous potassium phosphate. Structure elucidation of this group of compounds was accomplished using extensive 1D and 2D NMR spectroscopic studies, including H-1, C-13, COSY, NOESY, HSQC, and gHMBC experiments. The distinction between the linear structures I, II and the cyclic structure III was made mainly on the basis of the analysis of the cross peak between H-2 and H-4a in the COSY spectra, in combination with the long-range correlation between H-2 and C-4, 6 in the gHMBC spectra. Copyright (c) 2006 John Wiley & Sons, Ltd.

语种: 英语
WOS记录号: WOS:000238691300011
Citation statistics:
内容类型: 期刊论文
URI标识: http://ir.bjmu.edu.cn/handle/400002259/50141
Appears in Collections:北京大学药学院_期刊论文

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作者单位: 1.Peking Univ, State Key Lab Nat & Biomimet Drugs, Sch Pharmaceut Sci, Med & Hlth Anal Ctr, Beijing 100083, Peoples R China
2.Peking Univ, Dept Biol Chem, Sch Pharmaceut Sci, Beijing 100083, Peoples R China

Recommended Citation:
Li, Q,Yang, CH,Ge, ZM,et al. Structure elucidation of a novel group of dithiocarbamate derivatives using 1D and 2D NMR spectroscopy[J]. MAGNETIC RESONANCE IN CHEMISTRY,2006,44(7):720-723.
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