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Structure elucidation of a novel group of dithiocarbamate derivatives using 1D and 2D NMR spectroscopy
Li, Q1; Yang, CH1; Ge, ZM1; Li, RT1; Cui, YX1
关键词Nmr H-1 Nmr C-13 Nmr 2d Nmr Structural Elucidation Dithiocarbamates
刊名MAGNETIC RESONANCE IN CHEMISTRY
2006-07-01
DOI10.1002/mrc.1808
44期:7页:720-723
收录类别SCI
文章类型Article
WOS标题词Science & Technology
类目[WOS]Chemistry, Multidisciplinary ; Chemistry, Physical ; Spectroscopy
研究领域[WOS]Chemistry ; Spectroscopy
关键词[WOS]CANCER
英文摘要

Compounds 1-7 form a novel group of dithiocarbamates, first synthesized from the reaction of a series of primary amines with carbon disulfide and 3-bromo ethyl pyruvate in the presence of anhydrous potassium phosphate. Structure elucidation of this group of compounds was accomplished using extensive 1D and 2D NMR spectroscopic studies, including H-1, C-13, COSY, NOESY, HSQC, and gHMBC experiments. The distinction between the linear structures I, II and the cyclic structure III was made mainly on the basis of the analysis of the cross peak between H-2 and H-4a in the COSY spectra, in combination with the long-range correlation between H-2 and C-4, 6 in the gHMBC spectra. Copyright (c) 2006 John Wiley & Sons, Ltd.

语种英语
WOS记录号WOS:000238691300011
引用统计
被引频次:2[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/50141
专题北京大学药学院
北京大学药学院_化学生物学系
北京大学口腔医学院_儿童口腔科
作者单位1.Peking Univ, State Key Lab Nat & Biomimet Drugs, Sch Pharmaceut Sci, Med & Hlth Anal Ctr, Beijing 100083, Peoples R China
2.Peking Univ, Dept Biol Chem, Sch Pharmaceut Sci, Beijing 100083, Peoples R China
推荐引用方式
GB/T 7714
Li, Q,Yang, CH,Ge, ZM,et al. Structure elucidation of a novel group of dithiocarbamate derivatives using 1D and 2D NMR spectroscopy[J]. MAGNETIC RESONANCE IN CHEMISTRY,2006,44(7):720-723.
APA Li, Q,Yang, CH,Ge, ZM,Li, RT,&Cui, YX.(2006).Structure elucidation of a novel group of dithiocarbamate derivatives using 1D and 2D NMR spectroscopy.MAGNETIC RESONANCE IN CHEMISTRY,44(7),720-723.
MLA Li, Q,et al."Structure elucidation of a novel group of dithiocarbamate derivatives using 1D and 2D NMR spectroscopy".MAGNETIC RESONANCE IN CHEMISTRY 44.7(2006):720-723.
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