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学科主题: 药学
题名:
A stereocontrolled approach to (+/-)-nonactic acid
作者: Zhou, Yuedong1,2,3; Xu, Qiongfeng1,4; Zhai, Hongbin1,2,3,4
关键词: convergent ; nonactic acid ; racemic ; stereocontrolled ; synthesis
刊名: TETRAHEDRON LETTERS
发表日期: 2008-09-01
DOI: 10.1016/j.tetlet.2008.06.100
卷: 49, 期:36, 页:5271-5272
收录类别: SCI ; IC
文章类型: Article
WOS标题词: Science & Technology
类目[WOS]: Chemistry, Organic
研究领域[WOS]: Chemistry
关键词[WOS]: SILICON-CONTAINING COMPOUNDS ; (+)-METHYL NONACTATE ; ORGANIC-SYNTHESIS ; (&amp ; /-)-NONACTIC ACID ; PROPOSED STRUCTURE ; (+)-NONACTIC ACID ; (-)-NONACTIC ACID ; METHYL NONACTATE ; FEIGRISOLIDE-C ; ROUTE
英文摘要:

Racemic nonactic acid was efficiently constructed in a convergent, stereocontrolled fashion (7 steps, 27%). The present synthesis features a stereocontrolled 1,3-dione reduction with NaBH(4)/Et(2)B(OMe) and all acid-promoted stereospecific cyclization in the formation of 7. (C) 2008 Elsevier Ltd. All rights reserved.

语种: 英语
所属项目编号: 90713007 ; 20772141 ; 20625204 ; 20632030 ; 2006AA09Z405
项目资助者: NSFC ; MOST-863
WOS记录号: WOS:000258561400012
Citation statistics:
内容类型: 期刊论文
URI标识: http://ir.bjmu.edu.cn/handle/400002259/56887
Appears in Collections:北京大学药学院_期刊论文

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作者单位: 1.Chinese Acad Sci, Shanghai Inst Organ Chem, Lab Modern Synthet Organ Chem, Shanghai 200032, Peoples R China
2.Univ Sci & Technol China, Hefei Natl Lab Phys Sci Microscale, Hefei 230026, Anhui, Peoples R China
3.Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China
4.Peking Univ, Sch Pharmaceut Sci, State Key Lab Nat & Biomimet Drugs, Beijing 100083, Peoples R China

Recommended Citation:
Zhou, Yuedong,Xu, Qiongfeng,Zhai, Hongbin. A stereocontrolled approach to (+/-)-nonactic acid[J]. TETRAHEDRON LETTERS,2008,49(36):5271-5272.
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