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Simultaneous qualitative and quantitative determination of major polymethoxylated flavonoids in the leaves of Murraya paniculata by RRLC-DAD-ESI-MSn
Zhang, Jia-Yu; Li, Ning; Zhou, Yuan; Jiang, Yong; Tu, Peng-Fei
刊名ANALYTICAL METHODS
2012-10-01
DOI10.1039/c2ay25242b
4期:10页:3399-3406
收录类别SCI
文章类型Article
WOS标题词Science & Technology
类目[WOS]Chemistry, Analytical ; Food Science & Technology ; Spectroscopy
资助者Research Platform for Quality Standard of TCMs and Information System Building ; National S &amp ; T Major Project-Created Major New Drugs Projects ; Research Platform for Quality Standard of TCMs and Information System Building ; National S &amp ; T Major Project-Created Major New Drugs Projects
研究领域[WOS]Chemistry ; Food Science & Technology ; Spectroscopy
关键词[WOS]PERFORMANCE LIQUID-CHROMATOGRAPHY ; IONIZATION MASS-SPECTROMETRY ; ARRAY DETECTION ; CELL-LINES ; FRUIT ; PEEL
英文摘要

A rapid-resolution liquid chromatography-diode array detection-electrospray ionization tandem mass spectrometry (RRLC-DAD-ESI-MSn) method was established to identify and quantify the major bioactive constituents in the leaves of Murraya paniculata (L.) Jack. Seven of the main PMFs were determined by the RRLC method with detection wavelength at 330 nm in 30 minutes. The total PMFs in the samples ranged from 12.688 mg g(-1) to 54.997 mg g(-1). Meanwhile, sixteen PMFs could be identified from the complex extract of the leaves of M. paniculata by the RRLC-ESI-MS/MS method. The developed RRLC method was validated in terms of good linearity, precision and accuracy. The RRLC-ESI-MS/MS method was simple and useful for rapid identification of principal constituents in M. paniculata.

语种英语
所属项目编号2009ZX09308-04 ; 2009ZX09311-004
资助者Research Platform for Quality Standard of TCMs and Information System Building ; National S &amp ; T Major Project-Created Major New Drugs Projects ; Research Platform for Quality Standard of TCMs and Information System Building ; National S &amp ; T Major Project-Created Major New Drugs Projects
WOS记录号WOS:000309238300050
引用统计
被引频次:14[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/56969
专题北京大学药学院
作者单位Peking Univ, Hlth Sci Ctr, State Key Lab Nat & Biomimet Drugs, Sch Pharmaceut Sci, Beijing 100191, Peoples R China
推荐引用方式
GB/T 7714
Zhang, Jia-Yu,Li, Ning,Zhou, Yuan,et al. Simultaneous qualitative and quantitative determination of major polymethoxylated flavonoids in the leaves of Murraya paniculata by RRLC-DAD-ESI-MSn[J]. ANALYTICAL METHODS,2012,4(10):3399-3406.
APA Zhang, Jia-Yu,Li, Ning,Zhou, Yuan,Jiang, Yong,&Tu, Peng-Fei.(2012).Simultaneous qualitative and quantitative determination of major polymethoxylated flavonoids in the leaves of Murraya paniculata by RRLC-DAD-ESI-MSn.ANALYTICAL METHODS,4(10),3399-3406.
MLA Zhang, Jia-Yu,et al."Simultaneous qualitative and quantitative determination of major polymethoxylated flavonoids in the leaves of Murraya paniculata by RRLC-DAD-ESI-MSn".ANALYTICAL METHODS 4.10(2012):3399-3406.
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