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Preparative isolation and purification of acteoside and 2 ′-acetyl acteoside from Cistanches salsa (C.A. Mey.) G. Beck by highspeed counter-current chromatography
Li, L; Yang, FQ; Zhang, TY; Tu, PF; Wu, LJ; Ito, YC
关键词counter-current chromatography Cistanches salsa pharmaceutical analysis plant materials preparative chromatography acteoside acetylacteoside phenylethanoids glycosides
刊名JOURNAL OF CHROMATOGRAPHY A
2001-03-30
912期:1页:181-185
收录类别SCI
文章类型Article
WOS标题词Science & Technology
类目[WOS]Biochemical Research Methods ; Chemistry, Analytical
研究领域[WOS]Biochemistry & Molecular Biology ; Chemistry
英文摘要

High-speed counter-current chromatography (HSCCC) was applied to the separation and purification of phenylethanoid glycosides (PhGs) acteoside and 2 ′ -acetylacteoside from Cistanches salsa (C.A. Mey) G. Beck with a quaternary two-phase solvent system composed of ethyl acetate-n-butanol-ethanol-water (4:0.6:0.6:5, v/v). HPLC analyses of the CCC fractions revealed that the two main PhGs were over 98% purity. Their chemical structures were identified by LH NMR, C-13 NMR and MS. (C) 2001 Elsevier Science B.V. All rights reserved.

语种英语
WOS记录号WOS:000167589800020
Citation statistics
Cited Times:6[WOS]   [WOS Record]     [Related Records in WOS]
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/58521
Collection北京大学药学院
作者单位1.Beijing Inst New Technol Applicat, Beijing 100035, Peoples R China
2.NHLBI, Biophys Chem Lab, NIH, Bethesda, MD 20892 USA
3.Peking Univ, Sch Pharmaceut Sci, Beijing 100083, Peoples R China
4.Shenyang Pharmaceut Univ, Shenyang 110015, Peoples R China
Recommended Citation
GB/T 7714
Li, L,Yang, FQ,Zhang, TY,et al. Preparative isolation and purification of acteoside and 2 ′-acetyl acteoside from Cistanches salsa (C.A. Mey.) G. Beck by highspeed counter-current chromatography[J]. JOURNAL OF CHROMATOGRAPHY A,2001,912(1):181-185.
APA Li, L,Yang, FQ,Zhang, TY,Tu, PF,Wu, LJ,&Ito, YC.(2001).Preparative isolation and purification of acteoside and 2 ′-acetyl acteoside from Cistanches salsa (C.A. Mey.) G. Beck by highspeed counter-current chromatography.JOURNAL OF CHROMATOGRAPHY A,912(1),181-185.
MLA Li, L,et al."Preparative isolation and purification of acteoside and 2 ′-acetyl acteoside from Cistanches salsa (C.A. Mey.) G. Beck by highspeed counter-current chromatography".JOURNAL OF CHROMATOGRAPHY A 912.1(2001):181-185.
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