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Simultaneous determination of gallic acid, albiflorin, paeoniflorin, ferulic acid and benzoic acid in Si-Wu decoction by high-performance liquid chromatography DAD method
Sheng, YX; Li, L; Wang, Q; Guo, HZ; Guo, DA
关键词paeoniflorin albiflorin ferulic acid gallic acid benzoic acid Si-Wu decoction
刊名JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS
2005-04-01
DOI10.1016/j.jpba.2004.11.002
37期:4页:805-810
收录类别SCI
文章类型Article
WOS标题词Science & Technology
类目[WOS]Chemistry, Analytical ; Pharmacology & Pharmacy
研究领域[WOS]Chemistry ; Pharmacology & Pharmacy
关键词[WOS]MICELLAR ELECTROKINETIC CHROMATOGRAPHY ; CINNAMIC ACID ; SHIMOTSU-TO ; TANG ; GLYCYRRHIZIN ; CONSTITUENTS ; ELECTROPHORESIS ; CINNAMALDEHYDE ; &lt ; 6&gt ; -GINGEROL ; PUERARIN
英文摘要

A high-performance liquid chromatographic method was applied to the determination of gallic acid, albiflorin, paeoniflorin, ferulic acid and benzoic acid in Si-Wu decoction and other 13 combinations of the formula. These five compounds were analyzed simultaneously with a Zorbox SB C-18 column by gradient elution using 0.01% (v/v) phosphoric acid-acetonitrile as the mobile phase. The flow rate was 1 ml min(-1), and detection was set at 230 nm. The recovery of the method was in the range of 94.8-103.1%, and all the compounds showed good linearity (r > 0.9995) in a relatively wide concentration range. The result indicated that the content of these five compounds changed after decocting process. The contents of paeoniflorin, albiflorin, ferulic acid and gallic acid increased and that of benzoic acid decreased significantly. (c) 2004 Elsevier B.V. All rights reserved.

语种英语
WOS记录号WOS:000228783800025
引用统计
被引频次:34[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/58892
专题北京大学药学院
作者单位1.Peking Univ, Sch Pharmaceut Sci, Beijing 100083, Peoples R China
2.Peking Univ, Modern Res Ctr Tradit Chines Med, Beijing 100083, Peoples R China
推荐引用方式
GB/T 7714
Sheng, YX,Li, L,Wang, Q,et al. Simultaneous determination of gallic acid, albiflorin, paeoniflorin, ferulic acid and benzoic acid in Si-Wu decoction by high-performance liquid chromatography DAD method[J]. JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS,2005,37(4):805-810.
APA Sheng, YX,Li, L,Wang, Q,Guo, HZ,&Guo, DA.(2005).Simultaneous determination of gallic acid, albiflorin, paeoniflorin, ferulic acid and benzoic acid in Si-Wu decoction by high-performance liquid chromatography DAD method.JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS,37(4),805-810.
MLA Sheng, YX,et al."Simultaneous determination of gallic acid, albiflorin, paeoniflorin, ferulic acid and benzoic acid in Si-Wu decoction by high-performance liquid chromatography DAD method".JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS 37.4(2005):805-810.
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