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Efficient formation and cleavage of benzylidene acetals by sodium hydrogen sulfate supported on silica gel
Niu, Youhong; Wang, Ning; Cao, Xiaoping; Ye, Xin-Shan
关键词sodium hydrogen sulfate supported on silica gel protection deprotection benzylidene acetals carbohydrate
刊名SYNLETT
2007-08-13
DOI10.1055/s-2007-984903
13页:2116-2120
收录类别SCI ; IC ; CCR
文章类型Article
WOS标题词Science & Technology
类目[WOS]Chemistry, Organic
研究领域[WOS]Chemistry
关键词[WOS]SOLVENT-FREE CONDITIONS ; HETEROGENEOUS CONDITIONS ; SYNTHETIC METHODOLOGIES ; CARBONYL-COMPOUNDS ; CARBOHYDRATE-DERIVATIVES ; SELECTIVE DEPROTECTION ; N-BROMOSUCCINIMIDE ; SUGAR-DERIVATIVES ; PROTECTING GROUP ; CATALYST
英文摘要

NaHSO4 center dot SiO2 was used as an efficient heterogeneous catalyst for both the formation and the cleavage of benzylidene acetals. This catalyst is compatible with many functional or protective groups. Under different solvent systems, either the formation or the cleavage of benzylidene acetals was carried out smoothly in excellent yields and with good chemoselectivity.

语种英语
WOS记录号WOS:000249453200028
引用统计
被引频次:26[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/59078
专题北京大学药学院
作者单位1.Lanzhou Univ, Dept Chem, Lanzhou 730000, Peoples R China
2.Peking Univ, Sch Pharmaceut Sci, State Key Lab Nat & Biomimet Drugs, Beijing 100083, Peoples R China
3.Lanzhou Univ, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China
推荐引用方式
GB/T 7714
Niu, Youhong,Wang, Ning,Cao, Xiaoping,et al. Efficient formation and cleavage of benzylidene acetals by sodium hydrogen sulfate supported on silica gel[J]. SYNLETT,2007(13):2116-2120.
APA Niu, Youhong,Wang, Ning,Cao, Xiaoping,&Ye, Xin-Shan.(2007).Efficient formation and cleavage of benzylidene acetals by sodium hydrogen sulfate supported on silica gel.SYNLETT(13),2116-2120.
MLA Niu, Youhong,et al."Efficient formation and cleavage of benzylidene acetals by sodium hydrogen sulfate supported on silica gel".SYNLETT .13(2007):2116-2120.
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