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Isolation and structure characterization of evolimorutanin from the unripe fruits of Evodia rutaecarpa var. bodinieri
Yang Xiu-Wei; Hu, Zhang; Jun, Hu
关键词Evodia rutaecarpa (Juss.) Benth. var. bodinieri (Dode) Huang evolimorutanin limonin nuclear magnetic resonance (NMR)
刊名CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
2008-02-01
36期:2页:219-222
收录类别SCI
文章类型Article
WOS标题词Science & Technology
类目[WOS]Chemistry, Analytical
研究领域[WOS]Chemistry
英文摘要

A new and highly oxygenated limonoids compound, evolimorutanin 2, was isolated from the unripe fruits of Evodia rutaecarpa (Juss.) Benth. var. bodinieri (Dode) Huang (fructus evodiae) as a traditional Chinese medicine together with the known limonin 1. The chemical structure was elucidated by IR, MS, ID NMR(H-1 NMR, C-13 NMR and distorsionless enhancement by polarization transfer (DEPT)) and 2D NMR (H-1-H-1 COSY, heteronuclear single quantum coherence (HSQC) and hetero nuclear multiple bond coherence (HMBC)). Both limonin and evolimorutanin belong to nortriterpenoids compounds on the chemical structure and their substituents and stereochemistry in the rings A, A′, B, C, D were completely same, and their exclusive difference was the oxygenation in the ring E. In addition, the possible transformation route of evoli-morutanin from limonin via shihulimonin A is proposed.

语种中文
WOS记录号WOS:000254252200017
引用统计
被引频次:6[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/59266
专题北京大学药学院
作者单位Peking Univ, Sch Pharmaceut Sci, State Key Lab Nat & Biomimet Drugs, Beijing 100083, Peoples R China
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Yang Xiu-Wei,Hu, Zhang,Jun, Hu. Isolation and structure characterization of evolimorutanin from the unripe fruits of Evodia rutaecarpa var. bodinieri[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2008,36(2):219-222.
APA Yang Xiu-Wei,Hu, Zhang,&Jun, Hu.(2008).Isolation and structure characterization of evolimorutanin from the unripe fruits of Evodia rutaecarpa var. bodinieri.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,36(2),219-222.
MLA Yang Xiu-Wei,et al."Isolation and structure characterization of evolimorutanin from the unripe fruits of Evodia rutaecarpa var. bodinieri".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 36.2(2008):219-222.
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