IR@PKUHSC  > 北京大学药学院  > 化学生物学系
学科主题药学
The purification of glucose type glycosyl nitrate and the synthesis of spacer-armed N-acetyllactosamines and their dimers
Li, Q; Li, H; Su, B; Meng, XB; Cai, MS; Li, ZJ
关键词glycosyl nitrate glycosyl trichloroacemidate spacer-armed dimer
刊名CHINESE CHEMICAL LETTERS
2002-04-01
13期:4页:303-305
收录类别SCI
文章类型Article
WOS标题词Science & Technology
类目[WOS]Chemistry, Multidisciplinary
研究领域[WOS]Chemistry
英文摘要

3, 6-di-O-acetyl-4-O-(2, 3, 4, 6-tetra-O-acetyl-beta-D-galactopyranosyl)-2-azido-2-deoxy-beta-D-glucoppyranosyl nitrate could be separated from its mannose type isomer by glycosylation according to the reactivity difference of these two compounds. The pure glucose type nitrate can be converted to corresponding trichloroacemidate, which reacted with spacer arms in solution of CH2Cl2 with BF3.Et2O as promoters to give desired glycosides and dimers.

语种英语
WOS记录号WOS:000175155200009
Citation statistics
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/61502
Collection北京大学药学院_化学生物学系
作者单位1.Peking Univ, Sch Pharmaceut Sci, Dept Biol Chem, Beijing 100083, Peoples R China
2.Peking Univ, Natl Res Lab Nat & Biomimet Drugs, Beijing 100083, Peoples R China
Recommended Citation
GB/T 7714
Li, Q,Li, H,Su, B,et al. The purification of glucose type glycosyl nitrate and the synthesis of spacer-armed N-acetyllactosamines and their dimers[J]. CHINESE CHEMICAL LETTERS,2002,13(4):303-305.
APA Li, Q,Li, H,Su, B,Meng, XB,Cai, MS,&Li, ZJ.(2002).The purification of glucose type glycosyl nitrate and the synthesis of spacer-armed N-acetyllactosamines and their dimers.CHINESE CHEMICAL LETTERS,13(4),303-305.
MLA Li, Q,et al."The purification of glucose type glycosyl nitrate and the synthesis of spacer-armed N-acetyllactosamines and their dimers".CHINESE CHEMICAL LETTERS 13.4(2002):303-305.
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