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学科主题: 药学
题名:
The purification of glucose type glycosyl nitrate and the synthesis of spacer-armed N-acetyllactosamines and their dimers
作者: Li, Q; Li, H; Su, B; Meng, XB; Cai, MS; Li, ZJ
关键词: glycosyl nitrate ; glycosyl trichloroacemidate ; spacer-armed dimer
刊名: CHINESE CHEMICAL LETTERS
发表日期: 2002-04-01
卷: 13, 期:4, 页:303-305
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology
类目[WOS]: Chemistry, Multidisciplinary
研究领域[WOS]: Chemistry
英文摘要:

3, 6-di-O-acetyl-4-O-(2, 3, 4, 6-tetra-O-acetyl-beta-D-galactopyranosyl)-2-azido-2-deoxy-beta-D-glucoppyranosyl nitrate could be separated from its mannose type isomer by glycosylation according to the reactivity difference of these two compounds. The pure glucose type nitrate can be converted to corresponding trichloroacemidate, which reacted with spacer arms in solution of CH2Cl2 with BF3.Et2O as promoters to give desired glycosides and dimers.

语种: 英语
WOS记录号: WOS:000175155200009
Citation statistics:
内容类型: 期刊论文
URI标识: http://ir.bjmu.edu.cn/handle/400002259/61502
Appears in Collections:北京大学药学院_化学生物学系_期刊论文

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作者单位: 1.Peking Univ, Sch Pharmaceut Sci, Dept Biol Chem, Beijing 100083, Peoples R China
2.Peking Univ, Natl Res Lab Nat & Biomimet Drugs, Beijing 100083, Peoples R China

Recommended Citation:
Li, Q,Li, H,Su, B,et al. The purification of glucose type glycosyl nitrate and the synthesis of spacer-armed N-acetyllactosamines and their dimers[J]. CHINESE CHEMICAL LETTERS,2002,13(4):303-305.
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