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HPLC-DAD-MSn analysis and HPLC quantitation of chemical constituents in the traditional Chinese medicine formula Ya-tong-yi-li-wan
Liu, Ke-di; Qiao, Xue; Wang, Qing; Song, Wei; Guo, De-an; Ye, Min
刊名ANALYTICAL METHODS
2013
DOI10.1039/c3ay41054d
5期:19页:5241-5247
收录类别SCI
文章类型Article
WOS标题词Science & Technology
类目[WOS]Chemistry, Analytical ; Food Science & Technology ; Spectroscopy
研究领域[WOS]Chemistry ; Food Science & Technology ; Spectroscopy
关键词[WOS]PERFORMANCE LIQUID-CHROMATOGRAPHY ; TANDEM MASS-SPECTROMETRY ; GLYCYRRHIZA-URALENSIS ; BUFADIENOLIDES ; LICORICE ; IDENTIFICATION ; CHANSU
英文摘要

A combination of qualitative and quantitative methods was developed and validated to elucidate the chemical constituents in Ya-tong-yi-li-wan (YTYLW), a traditional Chinese medicine formula used for the treatment of toothache in China. Few reports are available on the chemical analysis of YTYLW, so far. For qualitative analysis, a method based on high-performance liquid chromatography coupled with diode-array detection and electrospray ionization tandem mass spectrometry (HPLC/DAD/ESI-MSn) was established. A total of 48 compounds in YTYLW were characterized, including 10 bufadienolides, 9 isoflavones, 7 chalcones, 7 saponins, 6 flavanones, 4 flavonols, 2 flavones, 2 coumarins, and 1 pterocarpan. For quantitative analysis, 12 major compounds in YTYLW were simultaneously determined by HPLC-UV at 270 nm in 9 batches of commercial products. Precision, reproducibility and accuracy of the method were fully validated. The method established in this study could be used for the quality control of YTYLW.

语种英语
WOS记录号WOS:000324489100041
引用统计
被引频次:4[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/61912
专题北京大学药学院
北京大学药学院_天然药物学系
北京大学第三临床医学院_护理部
北京大学精神卫生研究所_药房
作者单位Peking Univ, Sch Pharmaceut Sci, State Key Lab Nat & Biomimet Drugs, Beijing 100871, Peoples R China
推荐引用方式
GB/T 7714
Liu, Ke-di,Qiao, Xue,Wang, Qing,et al. HPLC-DAD-MSn analysis and HPLC quantitation of chemical constituents in the traditional Chinese medicine formula Ya-tong-yi-li-wan[J]. ANALYTICAL METHODS,2013,5(19):5241-5247.
APA Liu, Ke-di,Qiao, Xue,Wang, Qing,Song, Wei,Guo, De-an,&Ye, Min.(2013).HPLC-DAD-MSn analysis and HPLC quantitation of chemical constituents in the traditional Chinese medicine formula Ya-tong-yi-li-wan.ANALYTICAL METHODS,5(19),5241-5247.
MLA Liu, Ke-di,et al."HPLC-DAD-MSn analysis and HPLC quantitation of chemical constituents in the traditional Chinese medicine formula Ya-tong-yi-li-wan".ANALYTICAL METHODS 5.19(2013):5241-5247.
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