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Detection, characterization and identification of phenolic acids in Danshen using high-performance. liquid chromatography with diode array detection and electrospray ionization mass spectrometry
Liu, Ai-Hua; Guo, Hui; Ye, Min; Lin, Yan-Hua; Sun, Hang-Hao; Xu, Man; Guo, De-An
关键词phenolic acid salvia miltiorrhiza HPLC-DAD-ESI-MSn
刊名JOURNAL OF CHROMATOGRAPHY A
2007-08-17
DOI10.1016/j.chroma.2007.05.081
1161期:1-2页:170-182
收录类别SCI
文章类型Article
WOS标题词Science & Technology
类目[WOS]Biochemical Research Methods ; Chemistry, Analytical
研究领域[WOS]Biochemistry & Molecular Biology ; Chemistry
关键词[WOS]CHINESE MEDICINAL PREPARATIONS ; SALVIA-MILTIORRHIZA ; HPLC-DAD ; ROOTS ; QUANTIFICATION ; YUNNANENSIS ; METABOLITES ; TANSHINONES ; DEPSIDE
英文摘要

By using HPLC-diode array detection-electrospray ion trap tandem mass spectrometry (HPLC-DAD-ESI-MSn) in negative ion mode, we have analyzed the fragmentation pathways of 11 phenolic acids which were isolated from Danshen. Then the extract of Danshen was analyzed, and a total of 42 phenolic acids, including sixteen new minor constituents, were identified or tentatively identified for the first time. A new solidphase extraction (SPE) method, new HPLC separation method, new liquid chromatography (LC)-MS and LC-MSn (n = 3-5) data and proposed fragmentation pathways, LC retention time for phenolic acids are reported. (c) 2007 Elsevier B.V. All rights reserved.

语种英语
WOS记录号WOS:000248891500023
引用统计
被引频次:113[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/63044
专题北京大学药学院
作者单位1.Peking Univ, Sch Pharmaceut Sci, State Key Lab Nat & Biomimet Drugs, Beijing 100083, Peoples R China
2.Chinese Acad Sci, Shanghai Inst Biol Sci, Shanghai Inst Mat Med, Shanghai Res Ctr TCM Modernizat, Shanghai 201203, Peoples R China
推荐引用方式
GB/T 7714
Liu, Ai-Hua,Guo, Hui,Ye, Min,et al. Detection, characterization and identification of phenolic acids in Danshen using high-performance. liquid chromatography with diode array detection and electrospray ionization mass spectrometry[J]. JOURNAL OF CHROMATOGRAPHY A,2007,1161(1-2):170-182.
APA Liu, Ai-Hua.,Guo, Hui.,Ye, Min.,Lin, Yan-Hua.,Sun, Hang-Hao.,...&Guo, De-An.(2007).Detection, characterization and identification of phenolic acids in Danshen using high-performance. liquid chromatography with diode array detection and electrospray ionization mass spectrometry.JOURNAL OF CHROMATOGRAPHY A,1161(1-2),170-182.
MLA Liu, Ai-Hua,et al."Detection, characterization and identification of phenolic acids in Danshen using high-performance. liquid chromatography with diode array detection and electrospray ionization mass spectrometry".JOURNAL OF CHROMATOGRAPHY A 1161.1-2(2007):170-182.
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