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Synthesis of 6-(Bromomethyl)-4-methoxy-5,6,7,8-tetrahydropyrido[3,2-d]pyrimidin-2-ol from 6-Methylpyrimidine-2,4-diol
Liu Wei-dong2; Deng Xi-ling2; Zhang Zhi-li2; Wang Xiao-wei2; Liu Jun-yi1,2
关键词Heterocycle Carbanion Alkylation Reduction Cyclization
刊名CHEMICAL RESEARCH IN CHINESE UNIVERSITIES
2012-01-25
28期:1页:57-60
收录类别SCI
文章类型Article
WOS标题词Science & Technology
类目[WOS]Chemistry, Multidisciplinary
研究领域[WOS]Chemistry
关键词[WOS]INHIBITORS
英文摘要

6-(Bromomethyl)-4-methoxy-5,6,7,8-tetrahydropyrido[3,2-d]pyrimidin-2-ol(compound 9) was synthesized from 6-methylpyrimidine-2,4-diol(compound 1) through the crucial steps of 6-methyl alkylating and intramolecular cyclization. The assignment of the structure of compound 9 was performed by its spectral data, H-1 NMR, C-13 NMR, HMBC, and HRMS spectra.

语种英语
WOS记录号WOS:000300808300012
项目编号20672008 ; 20972011
资助机构National Natural Science Foundation of China ; PhD Foundation of the Ministry of Education of China
引用统计
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/63324
专题北京大学药学院
北京大学药学院_化学生物学系
作者单位1.Peking Univ, Sch Pharmaceut Sci, State Key Lab Nat & Biomimet Drug, Beijing 100191, Peoples R China
2.Peking Univ, Sch Pharmaceut Sci, Dept Biol Chem, Beijing 100191, Peoples R China
推荐引用方式
GB/T 7714
Liu Wei-dong,Deng Xi-ling,Zhang Zhi-li,et al. Synthesis of 6-(Bromomethyl)-4-methoxy-5,6,7,8-tetrahydropyrido[3,2-d]pyrimidin-2-ol from 6-Methylpyrimidine-2,4-diol[J]. CHEMICAL RESEARCH IN CHINESE UNIVERSITIES,2012,28(1):57-60.
APA Liu Wei-dong,Deng Xi-ling,Zhang Zhi-li,Wang Xiao-wei,&Liu Jun-yi.(2012).Synthesis of 6-(Bromomethyl)-4-methoxy-5,6,7,8-tetrahydropyrido[3,2-d]pyrimidin-2-ol from 6-Methylpyrimidine-2,4-diol.CHEMICAL RESEARCH IN CHINESE UNIVERSITIES,28(1),57-60.
MLA Liu Wei-dong,et al."Synthesis of 6-(Bromomethyl)-4-methoxy-5,6,7,8-tetrahydropyrido[3,2-d]pyrimidin-2-ol from 6-Methylpyrimidine-2,4-diol".CHEMICAL RESEARCH IN CHINESE UNIVERSITIES 28.1(2012):57-60.
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