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学科主题: 药学
题名:
Ligand-Free Pd(OAc)(2) Catalyzed Heck Reaction under Air
作者: Chen, Wei1; Yu, Miao2; Pan, Delin3; Jiao, Ning3
关键词: ligand-free ; Pd-catalyzed ; Heck reaction
刊名: CHINESE JOURNAL OF ORGANIC CHEMISTRY
发表日期: 2010-03-01
卷: 30, 期:3, 页:469-473
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology
类目[WOS]: Chemistry, Organic
研究领域[WOS]: Chemistry
关键词[WOS]: HYDROGEN SUBSTITUTION-REACTIONS ; ELECTRON-RICH OLEFINS ; COUPLING REACTIONS ; ARYL CHLORIDES ; VINYL ETHERS ; C-C ; PALLADIUM ; HALIDES ; ARYLATION ; SYSTEM
英文摘要:

Ligand-free Pd(OAc)(2) catalyzed Heck reaction under air was studied in this work. Iodobenzene, bromobenzene and their derivatives reacted smoothly with different alkenes in the presence of palladium acetate. The reactions were conducted under air in the absence of ligand. The effect of base, additives, solvents and catalysts on this transformation was investigated. The optimized reaction conditions were approved as: Pd(OAc)(2) (5 mol%), Ag2CO3 (0.6 equiv.), reflux in benzene or toluene under air.

语种: 中文
WOS记录号: WOS:000276472100024
Citation statistics:
内容类型: 期刊论文
URI标识: http://ir.bjmu.edu.cn/handle/400002259/63550
Appears in Collections:北京大学药学院_期刊论文

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作者单位: 1.Chinese PLA Postgrad Med Sch, Beijing 100853, Peoples R China
2.Chinese Peoples Liberat Army Gen Hosp, Dept Radiol, Beijing 100853, Peoples R China
3.Peking Univ, State Key Lab Nat & Biomimet Drugs, Sch Pharmaceut Sci, Beijing 100191, Peoples R China

Recommended Citation:
Chen, Wei,Yu, Miao,Pan, Delin,et al. Ligand-Free Pd(OAc)(2) Catalyzed Heck Reaction under Air[J]. CHINESE JOURNAL OF ORGANIC CHEMISTRY,2010,30(3):469-473.
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