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学科主题: 药学
题名:
Active Cobalt Catalyst for the Cleavage of Benzyl Ether
作者: Wang, Bo; Yin, Zhaojun; Li, Yangbing; Yang, Ting-Xiang; Meng, Xiang-Bao; Li, Zhong-Jun
刊名: JOURNAL OF ORGANIC CHEMISTRY
发表日期: 2011-11-18
DOI: 10.1021/jo2018284
卷: 76, 期:22, 页:9531-9535
收录类别: SCI ; IC ; CCR
文章类型: Article
WOS标题词: Science & Technology
类目[WOS]: Chemistry, Organic
研究领域[WOS]: Chemistry
关键词[WOS]: DE-O-BENZYLATION ; 3,4-DIMETHOXYBENZYL PROTECTING GROUPS ; SELECTIVE HYDROGENOLYSIS ; MPM 4-METHOXYBENZYL ; RANEY-NICKEL ; EFFICIENT ; SYSTEM ; MONOSACCHARIDES ; DEPROTECTION ; REDUCTION
英文摘要:

An improved method for the deprotection of benzyl ethers using a catalytic amount of Co-2(CO)(8) in the presence of Me2PhSiH and CO (1 atm) is described. The deprotection reaction is compatible with double bond or sulfur-containing substrates. The method also tolerates other functional groups, such as Ac, Piv, and Bz, and shows potential selectivity in perbenzylated monosaccharides.

语种: 英语
所属项目编号: 20732001 ; 21072016 ; 2012CB822100
项目资助者: National Natural Science Foundation of China ; National Basic Research Program of China
WOS记录号: WOS:000296754400039
Citation statistics:
内容类型: 期刊论文
URI标识: http://ir.bjmu.edu.cn/handle/400002259/63860
Appears in Collections:北京大学药学院_期刊论文

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作者单位: Peking Univ, State Key Lab Nat & Biomimet Drugs, Sch Pharmaceut Sci, Beijing 100191, Peoples R China

Recommended Citation:
Wang, Bo,Yin, Zhaojun,Li, Yangbing,et al. Active Cobalt Catalyst for the Cleavage of Benzyl Ether[J]. JOURNAL OF ORGANIC CHEMISTRY,2011,76(22):9531-9535.
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