IR@PKUHSC  > 北京大学药学院
学科主题药学
Facile one-pot synthesis of ethyl 3-alkyl-4-hydroxy-2-thioxothiazoildine-4-carboxylates
Ge, ZM; Li, Q; Zheng, SJ; Cheng, TM; Cui, YX; Li, RT
关键词ethyl 3-alkyl-4-hydroxy-2-thioxothiazolidine-4-carboxylate primary amine ethyl 3-bromo-2-oxopropanoate one-pot synthesis anhydrous potassium phosphate
刊名CHINESE JOURNAL OF CHEMISTRY
2006-03-01
24期:3页:381-385
收录类别SCI ; IC
文章类型Article
WOS标题词Science & Technology
类目[WOS]Chemistry, Multidisciplinary
研究领域[WOS]Chemistry
关键词[WOS]ACETYL THIAZOLIDINETHIONE REAGENT ; ALDOL REACTIONS ; ANALOGS ; ACID
英文摘要

Ethyl 3-alkyl-4-hydroxy-2-thioxothiazolidine-4-carboxylates were prepared in excellent yields from the reaction of corresponding primary amines with carbon disulfide and ethyl 3-bromo-2-oxopropanoate in the presence of anhydrous potassium phosphate in DMF at room temperature within 1 h. The structures of the highly functionalized products were corroborated spectroscopically JR, H-1 NMR, C-13 NMR, EI-MS) and by elemental analyses. A plausible mechanism for such type of cyclization was proposed.

语种英语
WOS记录号WOS:000235990900018
引用统计
被引频次:4[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/64177
专题北京大学药学院
作者单位Peking Univ, Sch Pharmaceut Sci, Beijing 100083, Peoples R China
推荐引用方式
GB/T 7714
Ge, ZM,Li, Q,Zheng, SJ,et al. Facile one-pot synthesis of ethyl 3-alkyl-4-hydroxy-2-thioxothiazoildine-4-carboxylates[J]. CHINESE JOURNAL OF CHEMISTRY,2006,24(3):381-385.
APA Ge, ZM,Li, Q,Zheng, SJ,Cheng, TM,Cui, YX,&Li, RT.(2006).Facile one-pot synthesis of ethyl 3-alkyl-4-hydroxy-2-thioxothiazoildine-4-carboxylates.CHINESE JOURNAL OF CHEMISTRY,24(3),381-385.
MLA Ge, ZM,et al."Facile one-pot synthesis of ethyl 3-alkyl-4-hydroxy-2-thioxothiazoildine-4-carboxylates".CHINESE JOURNAL OF CHEMISTRY 24.3(2006):381-385.
条目包含的文件
条目无相关文件。
个性服务
推荐该条目
保存到收藏夹
查看访问统计
导出为Endnote文件
谷歌学术
谷歌学术中相似的文章
[Ge, ZM]的文章
[Li, Q]的文章
[Zheng, SJ]的文章
百度学术
百度学术中相似的文章
[Ge, ZM]的文章
[Li, Q]的文章
[Zheng, SJ]的文章
必应学术
必应学术中相似的文章
[Ge, ZM]的文章
[Li, Q]的文章
[Zheng, SJ]的文章
相关权益政策
暂无数据
收藏/分享
所有评论 (0)
暂无评论
 

除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。