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学科主题: 药学
题名:
O,O-Dimethylthiophosphonosulfenyl bromide-silver triflate: a new powerful promoter system for the preactivation of thioglycosides
作者: Peng, Peng; Ye, Xin-Shan1
刊名: ORGANIC & BIOMOLECULAR CHEMISTRY
发表日期: 2011
DOI: 10.1039/c0ob00380h
卷: 9, 期:2, 页:616-622
收录类别: SCI ; IC ; CCR
文章类型: Article
WOS标题词: Science & Technology
类目[WOS]: Chemistry, Organic
研究领域[WOS]: Chemistry
关键词[WOS]: ONE-POT SYNTHESIS ; PRE-ACTIVATION PROTOCOL ; OLIGOSACCHARIDE SYNTHESIS ; GLYCOSIDIC LINKAGES ; ITERATIVE GLYCOSYLATION ; COMBINATORIAL SYNTHESIS ; BETA-MANNOPYRANOSIDES ; MEDIATED FORMATION ; BUILDING-BLOCKS ; COMPLEX TYPE
英文摘要:

O,O-Dimethylthiophosphonosulfenyl bromide (DMTPSB) in combination with silver triflate provides a powerful thiophilic promoter system. Both "armed" and "disarmed" thioglycoside glycosyl donors can be activated to form glycosidic linkages efficiently by the pre-activation protocol. The usefulness of this new promoter is illustrated by a successful iterative one-pot oligosaccharide assembly.

语种: 英语
所属项目编号: 20732001 ; 2009ZX09501-011
项目资助者: National Natural Science Foundation of China ; Ministry of Science and Technology of China
WOS记录号: WOS:000285749800041
Citation statistics:
内容类型: 期刊论文
URI标识: http://ir.bjmu.edu.cn/handle/400002259/65068
Appears in Collections:北京大学药学院_期刊论文

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作者单位: 1.Peking Univ, State Key Lab Nat & Biomimet Drugs, Beijing 100191, Peoples R China
2.Peking Univ, Sch Pharmaceut Sci, Beijing 100191, Peoples R China

Recommended Citation:
Peng, Peng,Ye, Xin-Shan. O,O-Dimethylthiophosphonosulfenyl bromide-silver triflate: a new powerful promoter system for the preactivation of thioglycosides[J]. ORGANIC & BIOMOLECULAR CHEMISTRY,2011,9(2):616-622.
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