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学科主题: 药学
题名:
Triphenylphosphine-N-Bromosuccinimide Mediated Chemoselective Cyclodehydration of Diols
作者: Zhao, Shuo; Wu, You; Sun, Qi; Cheng, Tie-Ming; Li, Run-Tao
关键词: cyclodehydration ; Ph3P ; NBS ; chemoselectivity ; cyclic ethers ; synthetic methods
刊名: SYNTHESIS-STUTTGART
发表日期: 2015-04-01
DOI: 10.1055/s-0034-1380132
卷: 47, 期:8, 页:1154-1162
收录类别: SCI ; IC ; CCR
文章类型: Article
WOS标题词: Science & Technology
类目[WOS]: Chemistry, Organic
研究领域[WOS]: Chemistry
关键词[WOS]: ONE-POT SYNTHESIS ; ANNONACEOUS ACETOGENINS ; VERSATILE PRECURSORS ; BIS-TETRAHYDROFURAN ; CYCLIC ETHERS ; CONSTRUCTION ; EFFICIENT ; ALCOHOLS ; SALTS ; DIETHOXYTRIPHENYLPHOSPHORANE
英文摘要:

A triphenylphosphine-N-bromosuccinimide mediated chemoselective cyclodehydration of diols is presented for the synthesis of polysubstituted tetrahydrofurans. 1,4-Diols and their derivatives can be rapidly cyclized to furnish tetrahydrofurans in high yields with one equivalent of Ph3P/NBS. Higher amount of Ph3P/NBS leads to the formation of dibromobutanes.

语种: 英语
所属项目编号: NSFC 20802004
项目资助者: National Science Foundation of China
WOS记录号: WOS:000352515100014
Citation statistics:
内容类型: 期刊论文
URI标识: http://ir.bjmu.edu.cn/handle/400002259/65674
Appears in Collections:北京大学药学院_期刊论文

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作者单位: Peking Univ, State Key Lab Nat & Biomimet Drugs, Sch Pharmaceut Sci, Beijing 100191, Peoples R China

Recommended Citation:
Zhao, Shuo,Wu, You,Sun, Qi,et al. Triphenylphosphine-N-Bromosuccinimide Mediated Chemoselective Cyclodehydration of Diols[J]. SYNTHESIS-STUTTGART,2015,47(8):1154-1162.
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