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学科主题: 药学
题名:
PdCl2 catalyzed efficient assembly of organic azides, CO, and alcohols under mild conditions: a direct approach to synthesize carbamates
作者: Ren, Long1; Jiao, Ning1,2
刊名: CHEMICAL COMMUNICATIONS
发表日期: 2014
DOI: 10.1039/c4cc00538d
卷: 50, 期:28, 页:3706-3709
收录类别: SCI ; IC ; CCR
文章类型: Article
WOS标题词: Science & Technology
类目[WOS]: Chemistry, Multidisciplinary
研究领域[WOS]: Chemistry
关键词[WOS]: FUSED-HETEROCYCLIC-COMPOUNDS ; OXIDATIVE CARBONYLATION ; CURTIUS REARRANGEMENT ; NITRENE TRANSFER ; THERAPEUTIC EFFICACY ; N-TOSYLHYDRAZONES ; TRANSITION-METALS ; CARBOXYLIC-ACIDS ; CARBON-MONOXIDE ; ARYL HALIDES
英文摘要:

A simple and readily available PdCl2 catalyzed carbamate synthesis method via isocyanate generation and application in situ has been developed. This chemistry provides an efficient and practical approach to synthesize carbamates from simple organic azides, CO atmosphere and alcohols. The broad scope, mild and neutral conditions, and only N-2 as the byproduct make this transformation very useful. Moreover, simple examples of modification of bioactivemolecules and construction of macrocycles were achieved through this protocol.

语种: 英语
所属项目编号: 21325206 ; 21172006 ; 20120001110013
项目资助者: National Science Foundation of China ; National Young Top-notch Talent Support Program ; PhD Programs Foundation of the Ministry of Education of China
WOS记录号: WOS:000332927500015
Citation statistics:
内容类型: 期刊论文
URI标识: http://ir.bjmu.edu.cn/handle/400002259/66502
Appears in Collections:北京大学药学院_期刊论文

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作者单位: 1.Peking Univ, Sch Pharmaceut Sci, State Key Lab Nat & Biomimet Drugs, Beijing 100191, Peoples R China
2.Nankai Univ, State Key Lab Elementoorgan Chem, Tianjin 300071, Peoples R China

Recommended Citation:
Ren, Long,Jiao, Ning. PdCl2 catalyzed efficient assembly of organic azides, CO, and alcohols under mild conditions: a direct approach to synthesize carbamates[J]. CHEMICAL COMMUNICATIONS,2014,50(28):3706-3709.
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