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学科主题: 药学
题名:
Synthesis and properties of a new SASRIN resin derivative: SASRIN-2-pyridylthiocarbonate (SASRIN-TOPCAT) resin
作者: Zhao, Peng; Yang, Zhen-Jun; Zhang, Liang-Ren; Zhang, Li-He
关键词: SASRIN resin derivative ; etherification ; solid-phase organic synthesis
刊名: TETRAHEDRON LETTERS
发表日期: 2008-04-28
DOI: 10.1016/j.tetlet.2008.03.017
卷: 49, 期:18, 页:2951-2955
收录类别: SCI
文章类型: Article
WOS标题词: Science & Technology
类目[WOS]: Chemistry, Organic
研究领域[WOS]: Chemistry
关键词[WOS]: SOLID-PHASE SYNTHESIS ; PROTECTED PEPTIDE-FRAGMENTS ; NEUTRAL CONDITIONS ; ALCOHOLS ; SUPPORT ; REAGENTS ; LINKERS ; AMIDES ; ETHERS
英文摘要:

A new SASRIN resin derivative, SASRIN TOPCAT resin, was synthesized by the reaction of SASRIN resin with 2-thiopyridyl chloroformate. The new resin can be used for the loading of alcohols and thiols under neutral conditions, and the release of alcohol from the resin is achieved by the treatment of 1% TFA in CH2Cl2 for 15-60 min. Compared to the other reported resins, SASRIN-TOPCAT resin is more suitable for the loading of alcohols in solid-phase organic synthesis. (c) 2008 Elsevier Ltd. All rights reserved.

语种: 英语
WOS记录号: WOS:000255420200022
Citation statistics:
内容类型: 期刊论文
URI标识: http://ir.bjmu.edu.cn/handle/400002259/67046
Appears in Collections:北京大学药学院_期刊论文

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作者单位: Peking Univ, Sch Pharmaceut Sci, State Key Lab Nat & Biomimet Drugs, Beijing 100083, Peoples R China

Recommended Citation:
Zhao, Peng,Yang, Zhen-Jun,Zhang, Liang-Ren,et al. Synthesis and properties of a new SASRIN resin derivative: SASRIN-2-pyridylthiocarbonate (SASRIN-TOPCAT) resin[J]. TETRAHEDRON LETTERS,2008,49(18):2951-2955.
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