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Simultaneous determination of six major stilbenes and flavonoids in Smilax china by high performance liquid chromatography
Shao, Bo; Guo, Hong-zhu; Cui, Ya-jun; Liu, Ai-hua; Yu, Hal-lan; Guo, Hui; Xu, Man; Guo, De-an
关键词Smilax china stilbenes flavonoids high performance liquid chromatography
刊名JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS
2007-07-27
DOI10.1016/j.jpba.2007.03.008
44期:3页:737-742
收录类别SCI
文章类型Article
WOS标题词Science & Technology
类目[WOS]Chemistry, Analytical ; Pharmacology & Pharmacy
研究领域[WOS]Chemistry ; Pharmacology & Pharmacy
关键词[WOS]CANCER CHEMOPREVENTIVE ACTIVITY ; ANTIOXIDANT ACTIVITY ; RESVERATROL ; CONSTITUENTS
英文摘要

A simple, sensitive and specific HPLC method was developed for simultaneous determination of the six major active constituents in Smilax china, namely taxifolin-3-O-alycoside (1), piceid (2), oxyresveratrol (3), engeletin (4), resveratrol (5) and scirpusin A (6), respectively. The samples were separated on an Aglient Zorbax XDB-C-18 column with gradient elution of acetonitrile and 0.02% phosphoric acid (v/v) at a flow rate of 1.0 ml/min and detected at 300 nm. The six target compounds were completely separated within 35 min. All calibration Curves showed good linearity (r(2) > 0.999) within test ranges. The reproducibility was evaluated by intra- and inter-day assays and R.S.D. values were less than 3.7%. The recoveries were between 93.7 and 103.0%. The method was successfully applied to the analysis of six constituents in 15 commercial samples of S. china. The results indicated that the developed HPLC assay was readily utilized as a quality control method for S. china. (c) 2007 Elsevier B.V. All rights reserved.

语种英语
WOS记录号WOS:000248738200015
引用统计
被引频次:28[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.bjmu.edu.cn/handle/400002259/68190
专题北京大学药学院
作者单位Peking Univ, Sch Pharmaceut Sci, State Key Lab Nat & Biomimet Drugs, Beijing 100083, Peoples R China
推荐引用方式
GB/T 7714
Shao, Bo,Guo, Hong-zhu,Cui, Ya-jun,et al. Simultaneous determination of six major stilbenes and flavonoids in Smilax china by high performance liquid chromatography[J]. JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS,2007,44(3):737-742.
APA Shao, Bo.,Guo, Hong-zhu.,Cui, Ya-jun.,Liu, Ai-hua.,Yu, Hal-lan.,...&Guo, De-an.(2007).Simultaneous determination of six major stilbenes and flavonoids in Smilax china by high performance liquid chromatography.JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS,44(3),737-742.
MLA Shao, Bo,et al."Simultaneous determination of six major stilbenes and flavonoids in Smilax china by high performance liquid chromatography".JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS 44.3(2007):737-742.
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